ArticleFoods (Basel, Switzerland)2026
Simultaneous Determination of 20 Sulfonamide Residues in Pork by Filter-Based Solid-Phase Extraction Cleanup and UHPLC-MS/MS.
Article in Foods (Basel, Switzerland), 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
To enable rapid and accurate determination of sulfonamide residues in animal-derived foods, a method was developed for the simultaneous analysis of 20 sulfonamides by ultra-high-performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS) combined with a FaVEx one-step cleanup column, using pork as a representative matrix. After extraction, samples were rapidly purified with a FaVEx-NM column and analysed in multiple reaction monitoring mode. Matrix-matched calibration was employed to compensate for matrix effects. The method showed good linearity for all analytes within their respective concentration ranges, with correlation coefficients (R
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