ArticleScience advances2026
Universal synthesis of high-entropy alloy nanostructures with femtosecond lasers.
Article in Science advances, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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9 authors.
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Abstract
High-entropy alloy nanostructures (HEA-NSs) hold promise in advanced catalysis and materials science, but lack a robust and universal synthetic strategy designed at an atomic level. Here, femtosecond lasers are used to prepare HEA-NSs, from single atoms to 100 nm nanoparticles, either free-standing or supported on a variety of substrates. Ultrafast excitation enables precise control over electron dynamics and instantaneously formed solvated electrons induce rapid, nonselective ion reduction ∼100 picoseconds post-irradiation, followed by stochastic atom nucleation and formation of atomically dispersed HEA-NSs through diffusion-controlled dynamics beyond nanoseconds. These processes are governed by the spatiotemporal confinement effect (STCE), with atomic diffusion restricted within nanoseconds, thereby enabling kinetic trapping of metastable nanoclusters with strict atomic-level dispersity. As a demonstration, FeCoNiRuPt achieved a peak power density of 2.1 W cm
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