ArticleACS materials Au2026
Liquid-Assisted Redox Synthesis Enables High-Yield Metastable Tetragonal Spinel Oxides.
Article in ACS materials Au, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Controlling phase selectivity for especially metastable multimetal oxides remains a central challenge, even though they are attractive for catalysis and energy conversion applications. The conventional synthesis method, like aqueous redox-precipitation, typically uses dilute reactant solutions, in which thermodynamic equilibrium favors stable products, limiting the selective synthesis of metastable phases. Here, we demonstrate a water-assisted reaction that plays a dual and decisive role in liquid-assisted redox synthesis (LRS) to obtain a metastable tetragonal cobalt-manganese spinel (CMO), rather than the readily formed cubic spinel. Limited initial hydration (0.5-1.5 mL) creates a highly concentrated microenvironment that enhances local acidity and shifts redox toward Mn
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