ArticleACS materials Au2026
Stoichiometry-Defined Phase Selection and Hydrophobic Molecular Sealing in Bioderived Deep Eutectic Solvents.
Article in ACS materials Au, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Deep eutectic solvents (DESs) are promising ionic media owing to their abundance, ionic conductivity, and wide potential windows. Bioderived DESs based on choline chloride are attractive due to their biodegradability and biocompatibility; however, their strong hygroscopicity leads to severe moisture uptake and instability. Here, we report a bioderived moisture-resistant DES of acetylcholine chloride as a hydrogen bond acceptor (HBA) and 3-phenylpropionic acid as a hydrophobic hydrogen bond donor. The hydrophobic component acts as a molecular seal, shielding the hygroscopic HBA from moisture through hydrogen-bond network reconfiguration. Systematic variation of the molar ratio reveals four distinct regimes: immiscible mixtures (1:1), saturated states (1:1.5), a homogeneous glass-forming liquid at the eutectic composition (1:2,
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