ArticleNanomaterials (Basel, Switzerland)2026
Structural, Morphological, and Textural Characterization of Ni- and Fe-Based KCC-1@C Hybrid Nanocomposites.
Article in Nanomaterials (Basel, Switzerland), 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Hybrid nanocomposites composed of dendritic fibrous nanosilica (DFNS) identified as KCC-1 and resorcinol-formaldehyde (RF) resin were synthesized via the polymer-assisted deposition (PAD) method for the incorporation of Ni and Fe in mono- and bimetallic configurations. The RF resin enabled uniform dispersion Fe-based and Ni-based nanoparticles through coordination with functional groups, while KCC-1 provided a high-surface-area, mesoporous support. A comprehensive structural and chemical characterization confirmed the formation of hematite in the Fe-based system; NiO and metallic Ni in the Ni-based material; and FeO, NiO and metallic Ni in the bimetallic composite, in the form of well-dispersed metal nanoparticles between 3-6 nm. Although a reduction in BET surface area was observed due to resin and metal loading, all nanocomposites retained mesoporous structures with Type IV isotherms and H3-type hysteresis, suitable for catalytic applications. The nanocomposites exhibited structural stability up to 800 °C under N
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