ArticleScience advances2026
Beyond solvothermal synthesis: construction of covalent organic frameworks at near-ambient conditions.
Article in Science advances, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
The development of a novel reaction synthesis method for covalent organic frameworks (COFs) under near-ambient conditions (NAC) is crucial for replacing the traditional solvothermal method and achieving gram-level production. However, to date, most of the reported synthesis methods rely on external devices to facilitate the chemical reactions, and COFs linkages are mainly focused on imine-linked COFs. Here, we report a straightforward NAC method for the synthesis of β-ketoamine linked COFs at 30°C under atmospheric conditions. A series of high crystallinity COFs with different topological structures and functional groups were achieved through this novel method. In addition, the reactions can be conducted in organic or aqueous acid solutions, and reactions on a gram-level scale can be accomplished. As a result, COF-β-KA-CF
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