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Pyridine-mediated tandem Knoevenagel condensation-decarboxylation: Chemoselectivity, mechanistic rationale, and discovery of a novel Lead(II) fumarate coordination polymer.
Article in Science progress. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
The pyridine-mediated tandem Knoevenagel condensation-decarboxylation of glyoxylic acid and malonic acid was investigated at 95 °C in neat anhydrous pyridine to establish the mechanistic basis of its strict substrate specificity and to characterise the coordination compound formed during lead(II) acetate-mediated product isolation. Fumaric acid was isolated in 92% yield with confirmed
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