ArticleJournal of applied crystallography2026
Gas-controlled capillary spinner for time-resolved powder X-ray diffraction under dynamic conditions.
Article in Journal of applied crystallography, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
A gas-controlled capillary spinner was developed for time-resolved powder X-ray diffraction measurements of crystalline materials under controlled atmospheres. This system enables continuous sample rotation with simultaneous gas control by integrating a gas-tight capillary cell, a magnetic fluid rotary feedthrough and a fast-response diaphragm valve, allowing diffraction measurements to be performed in rapidly changing environments. The system performance was evaluated using a standard Si powder sample, revealing that high-speed rotation significantly improves the uniformity of the diffraction peak intensity, with relative fluctuations reduced to <1% at speeds of ∼200 r min
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