ArticleJACS Au2026
Partial Hydrogenation of Aryl-Substituted Benzothiophenes, Benzofurans and Indoles by Photocatalytic Water Activation.
Article in JACS Au, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Transition-metal-catalyzed hydrogenation of heteroarenes provides direct access to three-dimensional, semisaturated scaffolds but remains particularly challenging for sulfur-containing compounds due to catalyst poisoning and undesired desulfurization. As a result, general methods for the direct catalytic hydrogenation of aryl-substituted benzothiophenes to the corresponding 2,3-dihydrobenzothiophenes (DHBTs) are lacking. Herein, we report a photocatalytic phosphine-mediated radical hydrogenation using water as the hydrogen source, enabling direct access to DHBTs. The generality of this method was demonstrated by a broad substrate scope, including diverse aryl- and heteroaryl-substituted substrates as well as related benzofurans, indoles, and other
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