ArticleACS omega2026
Controlling Iron Volatilization and Graphitization Through Pyrolysis in Benzoxazine Carbon Precursors.
Article in ACS omega, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Authors and funding
6 authors.
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Abstract
In this work, two benzoxazine networks, BisA-An and BisA-Fu, were synthesized with and without 15 wt % ferrocene to investigate the influence of polymer network structure on iron volatilization and subsequent graphitization behavior. It is hypothesized that increased network rigidity, associated with higher cross-link density, would suppress iron volatilization during pyrolysis to 1000 °C, thereby increasing the availability of catalytically active iron at graphitization temperatures (>700 °C). Iron evolution during pyrolysis was monitored using simultaneous thermal analysis-mass spectrometry (STA-MS), which revealed that the network with the least cross-linking functionality exhibited approximately an order of magnitude greater iron volatilization compared to networks with higher cross-linking functionality (from 1.27 × 10
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Registered trials
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