ArticleSmall methods2026
Hydrothermal-Assisted High-Yield Production of Large-Area Ti
Article in Small methods, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
MXenes, a family of two-dimensional transition metal carbides and nitrides, are promising for optoelectronic and shielding applications owing to their high electrical conductivity and tunable surface chemistry. However, their commercialization is hindered by poor oxidation stability, low-yield synthesis, hydrofluoric acid-based etching, and difficulty in producing large-area flakes. Here, we report an integrated hydrothermal etching and water-only delamination strategy for scalable production of high-quality, large-area MXene. Optimized hydrothermal etching enabled efficient Al removal while preserving multilayer MXene structure, providing an ideal precursor for the subsequent production of high-quality MXene flakes. Water-assisted delamination achieved few-layer flakes with a reproducible yield (∼80%). The resulting flakes exhibited a large average lateral size (∼5.0 µm) and high average electrical conductivity (18 067 S cm
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