ArticleSmall methods2026
Substrate-Assisted Flux Method for Robust Synthesis of Quantum-Grade Transition Metal Dichalcogenides.
Article in Small methods, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
High-quality two-dimensional transition metal dichalcogenides (TMDs) are crucial for exploring intrinsic electronic, optoelectronic, and quantum transport phenomena. Although flux-based growth produces ultrapure TMD crystals with low defect densities, its broader adoption is limited by long growth cycles, low yield, and extensive post-growth purification. Here, we report a substrate-assisted flux method (SAFM) that enables rapid synthesis of quantum-grade TMD single crystals with enhanced yield and no post-growth purification. By introducing sapphire into a Se-rich flux environment, SAFM enables vapor-mediated precursor delivery and vertical crystal growth under isothermal conditions, as supported by density functional theory calculations. Consequently, millimeter-scale WSe
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