ArticleOrganic process research & development2026
Numbering-Up Flow Electroreduction of α,β-Unsaturated Carbonyls from Gram to Pilot-Relevant Scale.
Article in Organic process research & development, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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4 authors.
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Abstract
A scalable flow electrochemical platform achieves up to 9.2 g/h productivity at a 100 g scale using an innovative three-electrode reactor design. Dual-sided cathodes enable 16 parallel channels across eight modules, maintaining 1 min residence time without reoptimization. The methodology processes diverse α,β-unsaturated carbonyl substrates (chalcones, heterocyclic enones, esters, ketones, carboxylic acids), explored 18 examples with broad functional group tolerance. The average productivity improvement across the substrates is 75-fold than the batch method with consistent performance from gram to pilot scale, establishing a cost-effective pathway for the electrochemical reduction reaction.
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