ArticleChemSusChem2026
Tunable Natural Deep Eutectic Solvents-Driven Fractionation of Olive Pomace in an Integrated Biorefinery: Linking Lignin Structural Tailoring to Carbohydrate Valorization and Biopolymer Production.
Article in ChemSusChem, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
The development of sustainable biorefineries requires integrated fractionation strategies capable of preserving carbohydrate streams while generating high-value lignin and bioactive fractions. In this study, olive pomace was valorized through a cascade approach combining optimized microwave-assisted extraction (MAE) of phenolic compounds, natural deep eutectic solvents (NADES)-enabled pretreatment, and chemo-enzymatic modification. MAE enabled recovery of a phenolic-rich fraction and reduced inhibitory compounds in the residual biomass, improving its suitability for downstream processing. The dephenolized substrate was subsequently subjected to NADES-based fractionation using acidic, alkaline, and neutral systems, including a laccase-assisted variant. Pretreatment performance depended on solvent chemistry. The acidic system (ChCl:lactic acid) achieved high delignification (≈68%) but produced restructured lignin with extensive β-O-4 cleavage. The alkaline NADES (K
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