ArticleMolecules (Basel, Switzerland)2026
Novel Magnetic Covalent Organic Frameworks Fabricated Through In Situ Synthesis and Assembly for the Efficient Extraction and Enrichment of Six Amide Herbicides.
Article in Molecules (Basel, Switzerland), 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Magnetic covalent organic frameworks (MCOFs) offer efficient adsorption via designable pore channels and active sites, along with rapid magnetic separation due to their intrinsic superparamagnetism. However, physical mixing or non-covalent assembly often leads to weak binding, causing the leaching or detachment of magnetic components during use, and compromises the well-defined crystallinity of the COF. In this study, we employed an in situ synthesis strategy at room temperature based on amidation and Schiff base reactions to fabricate a magnetic TAPT-DHTA-COF with good crystallinity and superparamagnetism. This material was used as a magnetic solid-phase extraction (MSPE) adsorbent to establish an MSPE-GC-MS/MS method for the determination of amide herbicides (AHs). The TAPT-DHTA-COF is rich in hydroxyl groups, which form strong hydrogen bonds with the polar AH molecules. In a green tea matrix, six AHs showed good linearity within the concentration range of 1-500 ng g
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