Evidence map›Paper›PMID 42263495›Full record

ArticleSolid state nuclear magnetic resonance2026

Single crystal sapphire spacers for in situ angle sensing and rotor stability diagnostics in MAS NMR.

Thomas M Osborn Popp, Charles G Mullen, Katrina L Brown, Joselyn B Dzieminski, Alexis M Scida, Jonathan A Tence, Konstantin Drallios, Jacqueline R Perodeau, Andrew J Nieuwkoop

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In one paragraph

Article in Solid state nuclear magnetic resonance, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

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0cells of the map it votes in
0citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

0 citing papers in PubMed.

No citing paper in PubMed yet.

4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

9 authors.

Thomas M Osborn PoppDepartment of Chemistry, Oregon State University, Corvallis, OR, 97330, United States. Electronic address: osbornpt@oregonstate.edu.
Charles G MullenPhoenix NMR, LLC, Loveland, CO, 80537, United States of America.
Katrina L BrownDepartment of Chemistry, Oregon State University, Corvallis, OR, 97330, United States.
Joselyn B DzieminskiDepartment of Chemistry and Chemical Biology, Rutgers, The State University of New Jersey, Piscataway, NJ, 08854, United States.
Alexis M ScidaDepartment of Chemistry, Oregon State University, Corvallis, OR, 97330, United States.
Jonathan A TenceDepartment of Chemistry, Oregon State University, Corvallis, OR, 97330, United States.
Konstantin DralliosDepartment of Chemistry, Oregon State University, Corvallis, OR, 97330, United States.
Jacqueline R PerodeauDepartment of Chemistry and Chemical Biology, Rutgers, The State University of New Jersey, Piscataway, NJ, 08854, United States.
Andrew J NieuwkoopDepartment of Chemistry and Chemical Biology, Rutgers, The State University of New Jersey, Piscataway, NJ, 08854, United States. Electronic address: an567@chem.rutgers.edu.

Funding

Atomic Resolution Characterization of Kindlin-2 Binding to Phosphatidylinositol Phosphatases in Lipid Bilayers by Solid-State NMRR01GM139905 · NIGMS · RUTGERS, THE STATE UNIV OF N.J. · PI NIEUWKOOP, ANDREW · 2021 to 2025
$1.7M
Acquisition of a 700 MHz NMR SpectrometerS10OD018518 · OD · OREGON STATE UNIVERSITY · PI BARBAR, ELISAR J · 2015 to 2015
$1.3M
NIGMS NIH HHS R01 GM139905NIH HHS S10 OD018518
6 · The paper itself

Abstract

Magic-angle spinning (MAS) NMR is predicated on the requirement that the rotor spin at the magic angle, yet in current practice, the effective rotor angle is not directly monitored during the experiment. Here we show that the use of a single-crystal sapphire spacer in a standard zirconia rotor provides a simple in situ sensor of the effective spinning angle and, remarkably, of rotor mechanical behavior as well. By monitoring the

Identifiers

PMID42263495
PMCPMC13290022

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.