ArticleAngewandte Chemie (International ed. in English)2026
Leveraging Molecular Weight Dispersity for Scalable, Precise Synthesis of Nanocylinders Via Quasi-Polymerization-Induced Self-Assembly.
Article in Angewandte Chemie (International ed. in English), 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
The scalable and precise synthesis of polymeric nanostructures represents a significant challenge due to the inherent trade-off between production efficiency and morphological control. Here, we introduce a quasi-polymerization-induced self-assembly (quasi-PISA) strategy that integrates in situ nucleation-growth kinetics to fabricate uniform cylindrical micelles from liquid crystalline block copolymers at high concentrations (up to 10 wt.%). Counterintuitively, we demonstrate that the broad molecular weight distribution of PISA, often considered a drawback, can be harnessed as a key variable for precise assembly. By modulating polymerization conditions, fibril lengths were well controlled from 100 nm to over 3 µm (with length dispersity < 1.10) without requiring pre-formed seeds. This enables the one-pot synthesis of triblock comicelles and gram-scale production. Rheological analysis revealed a scaling relationship between solution viscosity and fibril length (η ∝ L
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