Evidence map›Paper›PMID 42228488›Full record

ArticleJournal of synchrotron radiation2026

Synchrotron beamline setup enabling quasi-simultaneous PXRD and XANES measurements: case study of Fischer-Tropsch catalyst reduction at 60 bar.

Lipeng Yao, G Leendert Bezemer, Irene M N Groot, Oleg Konovalov, Maciej Jankowski

Abstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in Journal of synchrotron radiation, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

0numbers the graph read from it
0cells of the map it votes in
0citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

0 citing papers in PubMed.

No citing paper in PubMed yet.

4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors.

Lipeng YaoLeiden Institute of Chemistry, Leiden University, Einsteinweg 55, 2333 CC Leiden, The Netherlands.
G Leendert BezemerShell Global Solutions International BV, Energy Transition Campus Amsterdam, Grasweg 31, 1031 HW Amsterdam, The Netherlands.ORCID 0000-0002-7344-9250
Irene M N GrootLeiden Institute of Chemistry, Leiden University, Einsteinweg 55, 2333 CC Leiden, The Netherlands.ORCID 0000-0001-9747-3522
Oleg KonovalovESRF - The European Synchrotron, 71 Avenue des Martyrs, CS 40220, 38043 Grenoble Cedex 9, France.ORCID 0000-0002-0390-5900
Maciej JankowskiESRF - The European Synchrotron, 71 Avenue des Martyrs, CS 40220, 38043 Grenoble Cedex 9, France.ORCID 0000-0002-3796-0529

Funding

Nederlandse Organisatie voor Wetenschappelijk Onderzoek 015.013.024
6 · The paper itself

Abstract

Powder X-ray diffraction (PXRD) and X-ray absorption near-edge structure (XANES) spectroscopy are complementary techniques for probing cobalt-based (Co-based) Fischer-Tropsch synthesis (FTS) catalyst structures. PXRD reveals crystalline composition, while XANES provides information on coordination geometry and oxidation state. We developed a fast, automated measurement method, based on rapid selection of X-ray beam energy and a dedicated sample environment at beamline ID10 (ESRF), to combine in situ PXRD and XANES in a single experiment. This approach enables simultaneous monitoring of structural and electronic changes in Co-based FTS catalysts under in situ conditions up to 60 bar, offering a comprehensive view of catalyst dynamics.

Indexed as

beamline setupcatalyst structurecobalt reductionin situ PXRDin situ XANES

Identifiers

PMID42228488
PMCPMC13344594

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.