ArticleChemistry (Weinheim an der Bergstrasse, Germany)2026
Ultra-Wideline 2D Correlations Among Low-γ Species in Solid-State NMR via the Progressive Saturation of a Common Proton Reservoir.
Article in Chemistry (Weinheim an der Bergstrasse, Germany), 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Ultra-wideline nuclear magnetic resonance (NMR) spectra arising from large chemical shift anisotropy and/or quadrupolar broadening can span several MHz, rendering two-dimensional (2D) correlations between low-γ nuclei subject to these interactions exceptionally challenging. The limited pulse excitation bandwidth, poor sensitivity, and weak internuclear couplings make correlations between such spins nearly impossible in practice. To deal with such cases, this study introduces the PROgressive Saturation of the Protons Enhanced Correlation Technique (PROSPECT) experiment. PROSPECT correlates the powder spectra of low-γ nuclei through their independent dipolar interactions with a common
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