ArticleScientific reports2026
Mechanochemical optimization and scope of triple and multiple Sonogashira couplings of triethynylbenzene for conjugated porous polymer synthesis.
Article in Scientific reports, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Conjugated porous polymers are an important class of advanced materials whose precise synthesis is critical for applications in energy storage, photocatalysis, and next-generation electronics. Developing greener routes remains challenging due to solvent-intensive, energy-consuming methods. Ball milling has emerged as a powerful and versatile tool in organic synthesis and materials chemistry, offering a sustainable and solvent-free alternative to traditional solution-phase methods. Here, we report the optimization of a triple Sonogashira cross-coupling reaction under room-temperature ball-milling conditions, achieving high yields in short reaction times of 60 min. The optimal catalytic conditions involved PdCl
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