ArticleChemistry (Weinheim an der Bergstrasse, Germany)2026
Sonochemical Synthesis of Cobalt-Oxo-Cubanes as Redox-Active Platform for Proton-Coupled Electron Transfer.
Article in Chemistry (Weinheim an der Bergstrasse, Germany), 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Cobalt-oxo-cubanes (COCs) are efficient, earth-abundant analogs of the tetrameric manganese clusters of the natural photosystems. Yet, the synthesis of COCs remains a challenging affair. In this study, we report a simple sonochemical approach for the gram-scale synthesis of a series of pyridine-substituted COCs. The representative electronic variation via para-and meta-substituted pyridines provided a handle to evaluate the effect of the electronic nature of COCs on the overall redox activity. Furthermore, the electrochemical behavior of COC-XPy and its kinetics were investigated in a homogeneous system to provide insight into their solution-phase electrochemical behavior under neutral aqueous conditions. Cyclic voltammetry (CV) studies revealed a one-electron oxidation pathway at the [Co
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