ArticleACS electrochemistry2026
A Catalyst-Coated Mesoporous Carbon-Membrane Electrode Assembly for In Situ Soft X‑ray XPS and NEXAFS Studies of Electrocatalytic Interfaces.
Article in ACS electrochemistry, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
In situ soft X-ray spectroscopy provides direct insight into the electronic structure of electrocatalysts under realistic reaction conditions but remains technically challenging due to the need to combine aqueous electrochemistry with ultra-high-vacuum detection. Here, we present a mesoporous carbon-membrane working electrode assembly (WEA) that enables window-free in situ XPS and NEXAFS measurements during electrochemical reactions. The design integrates a Nafion proton-exchange membrane with a mesoporous carbon-ionomer contact layer and a thin IrO
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