ArticleACS omega2026
Sequential Effect of Reaction Temperature on Physical and Chemical Properties of ZnO Nanoparticles for Water Purification in a Photocatalytic Reactor.
Article in ACS omega, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
This study investigates the influence of reaction temperature on the coprecipitation synthesis of ZnO NPs and correlates their structural and morphological evolution with their photocatalytic performance. ZnO NPs synthesized at five temperatures, namely, 25, 35, 45, 55, and 65 °C, produced wurtzite-phase materials with varying crystallinities in the range of 77-89%. XRD, SEM, EDX, UV-vis spectroscopy, BET surface area measurement, and PL spectroscopy were used to obtain structural and compositional information about the synthesized NPs. The increase in temperature transforms the nanosheet-like structures into quasi-spherical particles with average crystallite sizes of 14-20 nm, as a function of variations in crystal defects and a high concentration of lattice distortions. Optical characterization revealed a red shift in the absorption edges, with a reduction in the bandgap (
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