ArticleSe pu = Chinese journal of chromatography2026
[Determination of perfluorinated compounds， antibiotics and pesticides in drinking water by automated solid phase extraction with ultra-performance liquid chromatography-tandem mass spectrometry].
Article in Se pu = Chinese journal of chromatography, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Emerging organic contaminants in drinking water, characterized by biological toxicity and environmental persistence. Developing effective strategies for monitoring and controlling these contaminants in drinking water has become an urgent need to ensure drinking water safety. However， the current detection technologies for emerging organic contaminants in drinking water mainly focus on analyzing a single type of pollutant， which increases in detection costs and fails to meet the urgent demand for rapid， multi-analyte screening in water quality monitoring. This study established a novel analytical method， which was based on the automatic solid phase extraction coupled with ultra-performance liquid chromatography-tandem mass spectrometry method （SPE-UPLC-MS/MS）， enabling the simultaneous detection of 30 contaminants with diverse physicochemical properties in drinking water. The 30 contaminants included perfluorinated compounds （PFCs）， antibiotics and pesticides. The water samples were pretreated automatically by an automatic solid phase extraction instrument， and then purified and enriched through an OASIS HLB solid phase extraction column. The 30 contaminants were separated on an ACQUITY UPLC HSS T3 column （100 mm×2.1 mm， 1.7 μm） with a gradient mobile phase consisting of 5 mmol/L ammonium acetate （containing 0.1% formic acid） and acetonitrile. The samples were analyzed and determined by the positive/negative switching mode of the electrospray ionization source， and quantified by the external standard method. The results showed that the 30 compounds had good linear relationships within the mass concentration ranges of 0.10-200.0 μg/L， and the correlation coefficients （
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