Evidence map›Paper›PMID 42086643›Full record

ArticleScientific reports2026

An archaeo-metabolomics approach for identifying cedar tar in archaeological samples: differentiating plant products and production processes.

Barbara Huber, Océane Pollet, Sahar B Kandil, Dennis Graen, Lou Spanneut, Daniel Giddings Vassão, Lindsay Mas-Normand, Céline Joliot, Elizabeth Roche, Sylvain Burri and 6 more

Abstract read
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Article in Scientific reports, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

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0citing papers in PubMed
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1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

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3 · Its place in the literature

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0 citing papers in PubMed.

No citing paper in PubMed yet.

4 · The record

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PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

16 authors.

Barbara HuberInstitute of Archaeological Science, University of Tübingen, Tübingen, Germany. huber@gea.mpg.de.
Océane PolletCentre de Recherche et d'Enseignement en Géosciences de l'Environnement (CEREGE), CNRS, IRD, INRAE, Collège de France, Aix-Marseille Université, Aix-en-Provence, France.
Sahar B KandilSchool of Chemistry, Cardiff University, Cardiff, UK.
Dennis GraenInstitute of Ancient Classics (Institut für Alterumswissenschaften), Friedrich-Schiller-Universität Jena, Jena, Germany.
Lou SpanneutCentre de Recherche et d'Enseignement en Géosciences de l'Environnement (CEREGE), CNRS, IRD, INRAE, Collège de France, Aix-Marseille Université, Aix-en-Provence, France.
Daniel Giddings VassãoDepartment of Biochemistry, Max Planck Institute for Chemical Ecology, Jena, Germany.
Lindsay Mas-NormandIMBE, CNRS, IRD, Aix Marseille Université, Avignon Université, Avignon, France.
Céline JoliotIMBE, CNRS, IRD, Aix Marseille Université, Avignon Université, Avignon, France.
Elizabeth RocheSchool of Chemistry, Cardiff University, Cardiff, UK.
Sylvain BurriTRACES UMR 5608 CNRS, Université Toulouse Jean Jaurès, Toulouse, France.
Aline DurandDepartment of History, CReAAH-UMR 6566, Le Mans Université, Le Mans, France.
Martine RegertCNRS, CEPAM, Université Côte d'Azur, Nice, France.
Ricardo FernandesDepartment of Archaeology, Max Planck Institute of Geoanthropology, Jena, Germany.
John A PickettSchool of Chemistry, Cardiff University, Cardiff, UK.
Gérald CulioliIMBE, CNRS, IRD, Aix Marseille Université, Avignon Université, Avignon, France.
Thibaut DevièseCentre de Recherche et d'Enseignement en Géosciences de l'Environnement (CEREGE), CNRS, IRD, INRAE, Collège de France, Aix-Marseille Université, Aix-en-Provence, France.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

The human ability to create manufactured substances is not a modern innovation. It began in the Middle Palaeolithic with the production of birch tar through dry distillation, a process of heating bark under low-oxygen conditions. Over time, this technological knowledge extended to other materials and purposes. Among these, cedar products became especially significant, valued in medicine, technology, cosmetics, and mummification. Yet, distinguishing cedar tar from other cedar products, such as resin or essential oil, has long challenged archaeological science due to their closely related chemical composition. Here we used a GC-MS-based metabolomics approach to identify chemical markers of cedar tar samples. Using modern Cedrus atlantica samples, we defined a set of diagnostic compounds (i.e. dihydro-ar-turmerone, cuparene, dihydrocurcumene, ar-himachalene and 1-methyl-3,5-diisopropylbenzene) that reveal both the cedar origin and the transformative process of dry distillation. As a proof of concept, these chemical markers were searched for and successfully detected in ancient Egyptian mummification balms (664-332 BCE), providing direct evidence for cedar tar use in embalming mixtures and new insights into ancient technologies and cultural practices.

Indexed as

ArchaeologyCedrusMetabolomicsGas Chromatography-Mass SpectrometryOils, VolatilePlant BarkOils, Volatile

Identifiers

PMID42086643
PMCPMC13144440

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