ArticleACS measurement science au2026
Liquid Chromatography-Charged Aerosol Detection for Characterization of Natural Toxin Reference Materials.
Article in ACS measurement science au, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Authors and funding
3 authors.
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Abstract
Developing certified reference materials (CRMs) for natural toxins is challenging due to the scarcity of raw materials, their high toxicity, and structural complexity. Typically, purified toxins in microgram to low milligram amounts are quantitated as stock solutions using quantitative nuclear magnetic resonance spectroscopy (qNMR) and then accurately diluted to their final concentrations. With the limited sensitivity of qNMR, additional techniques are required for homogeneity assessment, quantitation, and stability monitoring of less concentrated solutions. Liquid chromatography with charged aerosol detection (LC-CAD) enables nonspecific detection of compounds down to nanogram-on-column levels. A reversed-phase LC-CAD method was developed that also incorporates MS and DAD. Large volume injection programs were implemented to improve detection for samples at low μg mL
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