ArticleMaterials (Basel, Switzerland)2026
Oxidation Behavior of Direct Reduced Iron Powder During Ball-Milling Treatment.
Article in Materials (Basel, Switzerland), 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
High-quality direct reduced iron (DRI) powder is essential for applications in catalysis, adsorption, and electromagnetic materials. However, its tendency to reoxidize during processing presents a significant challenge. This study investigates the oxidation behavior of DRI powder during wet ball-milling treatment. Samples were characterized using chemical phase dissolution, X-ray diffraction (XRD), scanning electron microscopy with energy-dispersive X-ray spectroscopy (SEM-EDS), and X-ray photoelectron spectroscopy (XPS) to assess both bulk and surface oxidation. The results reveal that significant oxidation occurs during the wet grinding and subsequent processing stages, with the relative oxidation degree (ROD) of the iron powder increasing sharply from 6.08% to 26.81% as the grinding time is extended from 20 to 40 min. SEM-EDS analysis indicates that oxidation is particularly pronounced in particles smaller than 10 μm. XRD confirms the gradual transformation of Fe
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