Evidence map›Paper›PMID 41969265›Full record

ArticleSe pu = Chinese journal of chromatography2026

[Rapid determination of lubabegron residues in animal-derived foods by ultra performance liquid chromatography- tandem mass spectrometry].

Cheng Yang, Wei-Xia Zhu, Ya-Feng Liu, Hong-Wei Zhang, Wei Wei, Kai Hu

Abstract readEnglish Abstract
In one paragraph

Article in Se pu = Chinese journal of chromatography, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

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0citing papers in PubMed
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1 · What the graph read from it

What it found

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The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

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3 · Its place in the literature

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4 · The record

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5 · Who and what money

Authors and funding

6 authors.

Cheng YangZhengzhou Customs District,Zhengzhou 450003,China.
Wei-Xia ZhuZhengzhou Customs District,Zhengzhou 450003,China.
Ya-Feng LiuZhengzhou Customs District,Zhengzhou 450003,China.
Hong-Wei ZhangQingdao Customs District,Qingdao 266002,China.
Wei WeiZhengzhou Customs District,Zhengzhou 450003,China.
Kai HuHenan University of Chinese Medicine,Zhengzhou 450046,China.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Lubaberone (LUB) is the first U S Food and Drug Administration (FDA) approved feed additives for reducing gaseous emissions from animals or their wastes, and the intake of animal-derived foods is an important source of human exposure to LUB. However, the lack of applicable analytical methods makes it difficult for regulatory authorities to monitor LUB in animal-derived foods. There is an urgent need to establish efficient and accurate methods for the analysis of LUB in animal-derived foods. In this study, a method was developed for the determination of LUB from six types of typical animal-derived foods (beef, bovine liver, bovine fat, mutton, sheep liver and sheep fat) by ultra performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS). The effects of extraction solvent types, extraction methods, extraction time and purification cartridges on the recovery of LUB were investigated, and the optimal conditions for sample pretreatment were confirmed. The homogenized samples were extracted using 0.5% formic acid acetonitrile via ultrasonication for 10 min, and then filtered by high-speed centrifugation, and the extracted solution was cleaned using SPE with a PRiME HLB cartridge. The LUB was separated on a Shim-pack GIST C18-AQ chromatographic column (100 mm×2.1 mm, 2.7 μm) with 0.1% formic acid aqueous solution-0.1% formic acid acetonitrile as mobile phases at a flow rate of 0.3 mL/min, and detected in positive ion switching mode (ESI

Indexed as

Drug ResiduesFood ContaminationMeatTandem Mass SpectrometryAnimalsCattleChromatography, High Pressure LiquidFood AnalysisLiquid Chromatography-Mass SpectrometrySheepbeeflubabegron (LUB)solid-phase extraction (SPE)ultra performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS)

Identifiers

PMID41969265
PMCPMC13077532

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.