ArticleChemSusChem2026
Bis(oxalato)borate Salts as Safe and Fluorine-Free Alternatives to Conventional Supporting Electrolytes for Organic Electrosynthesis.
Article in ChemSusChem, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.
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1 citing paper in PubMed.
- Electrochemistry of Hypervalent Halogen Compounds.Accounts of chemical research · 2026Article
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3 authors.
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Abstract
Supporting electrolytes are indispensable in organic electrosynthesis, since they provide the ionic conductivity required for closing the electrical circuit. In combination with organic solvents, lithium or tetraalkylammonium salts of perchlorate, tetrafluoroborate, and hexafluorophosphate are typically employed. Although these salts exhibit good solubility and high electrochemical stability, there are known issues with chemical stability, safety, and sustainability. Therefore, problems are to be expected when transferring lab-scale innovations to industrial application, which is why sustainable and affordable alternatives with comparative performance are needed. In this context, we explored the use of commercially available lithium bis(oxalato)borate as potential candidate. In the present work, we compare the (electro)chemical properties to the standard salts in typical reaction media and characterize the performance in electrosynthesis using three different test cases. It was found that LiBOB can compete with LiClO
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