ArticleJACS Au2026
Scalable Miniemulsion Polymerization of Methyl Methacrylate (MMA) in Continuous Flow.
Article in JACS Au, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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4 authors.
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Abstract
A scalable methodology to perform miniemulsion polymerizations is demonstrated for the polymerization of methyl methacrylate (MMA). Scalability of the miniemulsification was achieved by using a spinning disk reactor, which provides the required energy input to form a metastable emulsion, yielding miniemulsion droplets with an average size of 154 nm and a PDI of 0.17. Polymerization proceeds likewise in a scalable fashion, achieved by using agitated continuous flow reactors, which effectively prevent reactor fouling, a problem that typically limits emulsion polymerization in continuous flow. For the MMA miniemulsion process, synthesis of over 100g of polymer particles with well-defined particle distributions (the average polymer particle size, obtained after polymerization in the ATR reactor following emulsification using the SDR, was 170 nm with a PDI of 0.10) has been achieved, and operation of the designed reactor setup is stable over an entire workday. The space-time yield of the miniemulsion was found to be 53 g/Lh, significantly outperforming previous methods of miniemulsion polymerization.
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