ArticleThe Analyst2026
High- and low-field NMR in binary solvent gradients.
Article in The Analyst, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Authors and funding
5 authors.
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Abstract
We introduce composition gradients of the solvent as a powerful new dimension for NMR analysis on both high-field and benchtop instruments. Taking advantage of the differences in the density and miscibility of binary solvent mixtures with different compositions, we layer two solutions at opposite extremes of the compositional range in an NMR tube. The diffusion of the layers into each other establishes a continuous variation in the solvent composition across the sample. Spatially resolved analysis of the sample using either chemical shift imaging (CSI) on high-field NMR instruments or physical movement of the sample (benchtop instruments) enables analysis of chemical systems as a function of the solvent composition. In high field, we determine the p
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Registered trials
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