ArticleACS omega2026
Coordination Chemistry at the Hard-Soft Interface: Phosphine Oxide-Based Rare Earth/Transition Metal Complexes.
Article in ACS omega, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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6 authors.
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Abstract
A series of monometallic Al-(III), Sm-(III), Dy-(III), Er-(III), and Yb-(III) complexes, featuring tetraphenyldiphosphine monoxide (PPO) as a ligand, were synthesized and characterized. These complexes served as precursors for the construction of heterobimetallic rare earth (RE)/transition metal (TM) assemblies. Attempts to introduce soft TMs, such as Cu-(I) and Au-(I), into the preformed RE-PPO synthons predominantly afforded equilibrium-driven TM-based POP species, underscoring the challenges of incorporating hard and soft metal centers directly. This observation led to an alternative route employing a presynthesized Mo-PPO synthon, which led to the successful formation of RE/Mo heterobimetallic complexes upon addition of the RE ions. The molecular structures of both mono- and heterobimetallic species were strongly influenced by the solvent environment. Notably, reactions in dichloromethane, a noncoordinating solvent, yielded RE
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