ArticleACS catalysis2025
Nickel-Catalyzed Enantioselective Diboration of 1,2-Dihydropyridines: Application and Insight into the Selectivity and Mechanism.
Article in ACS catalysis, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
1,2-Dihydropyridine was found to undergo enantioselective nickel-catalyzed 1,4-diboration with exclusive regio- and diastereoselectivity employing a monodentate chiral phosphine ligand. The products were found to undergo regioselective allylic Suzuki-Miyaura cross-coupling with various electrophiles with high diastereospecificity. Insights into 1,4-diboration regioselectivity as well as putative reaction intermediates were obtained through NMR experimentation and computational studies.
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