Evidence map›Paper›PMID 41658219›Full record

ArticleACS omega2026

Corn starch/Carboxymethyl Cellulose Films: Influence of Citric Acid on Water Susceptibility, Morphological and Tensile Properties.

Michele Barbosa Santos, José Antonio da Silva Souza, Verônica Scarpini Cândido, Jordan Del Nero, Waldomiro Paschoal Junior, Ana Aurea Barreto Maia, Bruno Marques Viegas, Severino Alves Junior, Carlos Alberto Brito da Silva, Marcos Vinícius da Silva Paula

Abstract read
In one paragraph

Article in ACS omega, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.

0numbers the graph read from it
0cells of the map it votes in
3citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

3 citing papers in PubMed.

  1. Article
  2. Article
  3. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

10 authors.

Michele Barbosa SantosFaculdade de Engenharia de Materiais, Universidade Federal do Pará, Ananindeua 67130-660, Brasil.
José Antonio da Silva SouzaPrograma de Pós-Graduação em Engenharia de Recursos Naturais da Amazônia, Universidade Federal do Pará, Belém 66079-420, Brasil.
Verônica Scarpini CândidoFaculdade de Engenharia de Materiais, Universidade Federal do Pará, Ananindeua 67130-660, Brasil.
Jordan Del NeroFaculdade de Física, Universidade Federal do Pará, Belém 66075-110, Brasil.
Waldomiro Paschoal JuniorFaculdade de Física, Universidade Federal do Pará, Belém 66075-110, Brasil.
Ana Aurea Barreto MaiaFaculdade de Engenharia Química, Universidade Federal do Pará, Belém 66075-110, Brasil.
Bruno Marques ViegasPrograma de Pós-Graduação em Biotecnologia, Universidade Federal do Pará, Belém 66075-110, Brasil.
Severino Alves JuniorDepartamento de Química Fundamental, Universidade Federal de Pernambuco, Recife 50740-560, Brasil.ORCID https://orcid.org/0000-0002-8092-4224
Carlos Alberto Brito da SilvaPrograma de Pós-Graduação em Ciência e Engenharia de Materiais, Universidade Federal do Pará, Ananindeua 67130-660, Brasil.ORCID https://orcid.org/0000-0002-7084-8491
Marcos Vinícius da Silva PaulaFaculdade de Engenharia de Materiais, Universidade Federal do Pará, Ananindeua 67130-660, Brasil.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

The present study aimed to produce and characterize corn starch/carboxymethyl cellulose (TPC/CMC) films cross-linked with different concentrations of citric acid (CA). The films were obtained by solvent evaporation (casting solution) with 5, 10, 15, and 20% citric acid relative to the CMC mass (TPC/CMC-CA-0 to 20). They were qualitatively evaluated for visual aspects, swelling, moisture content, and solubility, and characterized by Fourier transform infrared spectroscopy (FTIR), thickness, and scanning electron microscopy (SEM). The results allowed us to evaluate the cross-linking effect promoted by citric acid. Visually, all films showed excellent optical transparency. FTIR spectroscopy demonstrated the formation of ester groups, indicative of cross-linking of the TPC-CMC films. SEM images revealed a homogeneous surface morphology without porosity in the films with CA. The addition of CA to the TPC-CMC films reduced water swelling, moisture absorption, and permeation. Additionally, the insertion of citric acid promoted an improvement in the tensile strength of TPC-CMC from 6.07 to 8.39 MPa for TPC-CMC/CA-15. This same trend was obtained with an increase of around 115% for the modulus in the TPC-CMC/CA-15 film compared to the film without CA. These results were due to cross-linking promoted by CA which produces a more cohesive material and thus increases the modulus and tensile strength. Thus, our results demonstrate that the cross-linking promoted by CA in TPC-CMC films has a profound influence on their water susceptibility and tensile properties.

Identifiers

PMID41658219
PMCPMC12878765

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.