ArticleJournal of the American Chemical Society2026
An Organoborate Monoxide Radical.
Article in Journal of the American Chemical Society, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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5 authors.
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Abstract
The boron monoxide radical has emerged as a fascinating molecule and a short-lived intermediate, previously observed only under matrix isolation conditions. In this study, we report the successful synthesis and characterization of a stable organic boron monoxide radical, achieved through the reaction of a diboron (6) dianion with nitric oxide (NO). This oxygen-centered radical is uniquely functionalized and stabilized by a triaryl-substituted boryl group. Comprehensive characterization was performed using various spectroscopic and structural techniques, including electron paramagnetic resonance (EPR) spectroscopy and single-crystal X-ray diffraction analysis. Remarkably, this oxygen-centered radical is stabilized by the K cation and exhibits significant stability under argon at room temperature, showing no self-dimerization even when heated or exposed to UV light. However, it can dimerize to form peroxide species when the K cation is fully encapsulated. Furthermore, it can mimic transition-metal complexes by mediating NO coupling to form a boryl hyponitrite (N
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