ArticleJournal of food science2026
Ultrasound-Assisted Extraction Using a 3D-Printed Device Functionalized With SPE Sorbent for UHPLC-DAD Analysis of Pesticide Residues in Honey.
Article in Journal of food science, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.
What it found
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The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.
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Who cites it
1 citing paper in PubMed.
- Ultrasound-Assisted Extraction Using a 3D-Printed Device Functionalized With SPE Sorbent for UHPLC-DAD Analysis of Pesticide Residues in Honey.Journal of food science · 2026Article
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Authors and funding
3 authors.
Funding
Abstract
The presence of pesticide residues in honey represents a significant concern for food safety and public health, underscoring the need for advanced analytical techniques capable of ensuring accurate detection and effective food control. In this study, a stereolithographically 3D-printed device coated with the solid-phase extraction (SPE) sorbent Oasis MCX was developed for the ultrasound-assisted extraction (UAE) of pesticide residues in honey, followed by ultra-high performance liquid chromatography with diode array detection (UHPLC-DAD) analysis. Variables that affect the performance of the 3D-printed extraction (i.e., design and fabrication of 3D-printed device, SPE resin, elution solution, pH, and ultrasonic conditions) and the chromatographic analysis were systematically evaluated. The optimized methodology allowed the simultaneous determination of five pesticides: azoxystrobin (AZO), carbaryl (CAR), pirimicarb (PIR), thiacloprid (THC), and thiamethoxam (THI). Chromatographic separation was completed in less than 15 min using a KinetexXB-C18 column (2.6 µm, 100 Å, 100 × 3 mm), with a mobile phase consisting of methanol and 0.1% formic acid (pH 3.35). The proposed methodology showed satisfactory agreement compared with commercial QuEChERS dispersive SPE kits. The developed method demonstrated good linearity up to 100 mg L
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