ArticleThe Journal of organic chemistry2025
Copper-Catalyzed 1,2-Diazidation and 1,2-Azidooxygenation of 1,3-Dienes: Three Divergent Protocols Using Zhdankin's Reagent.
Article in The Journal of organic chemistry, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
A series of three divergent protocols for the copper-catalyzed azidation of 1,3-dienes using iodine(III) Zhdankin's reagent is reported. This strategy features protocols for 1,2-diazidation, two-component 1,2-azidooxygenation, and three-component 1,2-azidooxygenation of 1,3-dienes in highly chemo-, regio-, and site-selective fashion under mild conditions. Excellent to fair yields are reported for a variety of activated and unactivated 1,3-diene systems with a range of substitution patterns. Additionally, mechanistic investigations are included to provide insights into the underpinnings for the divergence of these protocols and the component requirements.
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