ArticleJournal of synchrotron radiation2026
Modular reactor for in situ X-ray scattering, spectroscopy and ATR-IR studies of solvothermal nanoparticle synthesis.
Sani Y Harouna-Mayer, Melike Gumus Akcaalan, Jagadesh Kopula Kesavan, Tjark R L Groene, Lars Klemeyer, Sarah Alexandra Hussak, Lukas Grote, Davide Derelli, Francesco Caddeo, Cecilia Zito and 7 more
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In one paragraphArticle in Journal of synchrotron radiation, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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17 authors.
Melike Gumus AkcaalanUniversity of Hamburg, Institute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures (ChyN), Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0000-0003-2675-5893 Jagadesh Kopula KesavanUniversity of Hamburg, Institute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures (ChyN), Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0000-0002-0591-2493 Tjark R L GroeneUniversity of Hamburg, Institute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures (ChyN), Luruper Chaussee 149, 22761 Hamburg, Germany.
Lars KlemeyerUniversity of Hamburg, Institute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures (ChyN), Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0000-0003-1103-8103 Sarah Alexandra HussakUniversity of Hamburg, Institute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures (ChyN), Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0009-0005-8051-9746 Lukas GroteUniversity of Hamburg, Institute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures (ChyN), Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0000-0002-7023-5978 Davide DerelliUniversity of Hamburg, Institute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures (ChyN), Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0009-0004-0719-8651 Francesco CaddeoUniversity of Hamburg, Institute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures (ChyN), Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0000-0002-2909-5379 Cecilia ZitoUniversity of Hamburg, Institute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures (ChyN), Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0000-0001-5596-012X Paul StützleUniversity of Hamburg, Institute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures (ChyN), Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0009-0007-6625-319X Dorota SpeerUniversity of Hamburg, Institute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures (ChyN), Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0009-0007-2063-5993 Blanka DetlefsESRF - The European Synchrotron, 71 Avenue des Martyrs, CS40220, 38043 Grenoble, France.ORCID 0000-0002-9768-647X Yannik AppiariusUniversity of Hamburg, Department of Chemistry, Martin Luther King Platz 6, 20146 Hamburg, Germany.ORCID 0000-0002-9849-6950 Axel Jacobi von WangelinUniversity of Hamburg, Department of Chemistry, Martin Luther King Platz 6, 20146 Hamburg, Germany.ORCID 0000-0001-7462-0745 Dorota KoziejUniversity of Hamburg, Institute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures (ChyN), Luruper Chaussee 149, 22761 Hamburg, Germany.
Funding
Bundesministerium für Bildung und Forschung 05K20GUABundesministerium für Bildung und Forschung 05K22GU7Deutsche Forschungsgemeinschaft 390715994European Research Council 818941
6 · The paper itselfAbstract
Understanding the chemical processes that occur during the solvothermal synthesis of functional nanomaterials is essential for their rational design and optimization for specific applications. However, these processes remain poorly understood, primarily due to the limitations of conventional ex situ characterization techniques and the technical challenges associated with in situ studies, particularly the design and implementation of suitable reactors. Here, we present a versatile reactor suitable for in situ X-ray scattering, X-ray spectroscopy and infrared spectroscopy studies performed during solvothermal synthesis under autoclave-like, inert conditions. The reactor enables precise control of the temperature between -20°C and 200°C, pressure up to 8 bar, magnetic stirring, and injection of gas or liquids. The reactor's capabilities are demonstrated by comprehensively studying the solvothermal synthesis of magnetite nanoparticles from iron acetylacetonate in benzyl alcohol through in situ X-ray scattering and spectroscopy, and attenuated total reflection infrared (ATR-IR) spectroscopy.
Indexed as
colloidal nanostructurecomplementary in situ X-ray absorption spectroscopy and X-ray scatteringmultimodal in situ infrared spectroscopyreactor designsolvothermal synthesis
Identifiers
PMID41334684
PMCPMC12809455
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