ArticleACS omega2025
Pd-Catalyzed Hydroxylation of Aryl Halides under Air and in Eco-Friendly Solvent.
Article in ACS omega, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Authors and funding
7 authors.
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Abstract
A Pd-catalyzed synthesis of phenols in 10% aqueous poly-(ethylene glycol)-2000 (PEG) under an air atmosphere is reported. The reaction proceeds with NaOH as opposed to other BippyPhos/Pd systems in organic solvents that rely on more expensive and reactive CsOH. The reported method converts aryl chlorides, bromides, and iodides with a variety of functional groups at 90 °C to the corresponding phenols in moderate to excellent yields. Due to the aerobic atmosphere, these conditions also oxidize benzyl alcohol substituents to the corresponding aldehyde.
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Registered trials
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