ArticleACS electrochemistry2025
Highly Corrugated Ni Films Electrodeposited onto Boron Doped Diamond Electrodes for Alkaline Water Electrolysis.
Article in ACS electrochemistry, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Ni-based electrocatalysts are among the most active materials for the hydrogen evolution reaction (HER) in alkaline media. In this work, we demonstrate the ability to use films of boron-doped diamond (BDD), a stable and corrosion-resistant electrode material, as a support for highly textured Ni films. Our approach is based on the electrodeposition of NiCu alloy thin-films, followed by electrochemical dealloying. The structure and composition of the electrocatalysts were characterized using scanning electron microscopy, X-ray diffraction, and X-ray photoelectron spectroscopy. In pH 13 KOH, a dealloyed Ni catalyst corresponding to an initial NiCu composition of 68% Ni, gave a HER overpotential at 10 mA cm
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