ArticleACS nanoscience Au2025
Complex Intergrowth LnCuOSe Nanocrystals via Precursor-Directed Colloidal Synthesis.
Article in ACS nanoscience Au, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Colloidal synthesis of multielement nanocrystals demands precise control over precursor reactivity and compatibility. These challenges are amplified when combining elements that span the periodic table, which has limited the complexity of crystal structures and compositions that are readily accessible in solution. Intergrowth structures, which feature alternating layers with distinct compositions and crystallographic motifs, have proven particularly challenging to access in nanocrystalline forms. Here, we present a direct, solution-phase synthesis of LnCuOSe intergrowth nanocrystals incorporating six different lanthanide cations (Ln = La, Ce, Pr, Nd, Sm, and Eu). These nanocrystals exhibit a consistent anisotropic nanoflower morphology, reflecting the layered crystal structure of alternating Cu-Se and Ln-O planes. The synthesis leverages a preformed lanthanide-selenium interaction in a coordination complex precursor that thermally decomposes to yield the quaternary product. Formation proceeds via a crystalline Cu
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