ArticleSe pu = Chinese journal of chromatography2025
[Simultaneous determination of 15 bisphenols in prepared dishes by soild phase extraction purification-ultra performance liquid chromatography-tandem mass spectrometry].
Article in Se pu = Chinese journal of chromatography, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Bisphenols （BPs）， which include bisphenol A and its analogs （such as bisphenol S， bisphenol AF， and bisphenol B）， are chemical substances that are synthesized artificially. BPs are used in epoxy resins and polycarbonate plastics and are widely found in food packaging and beverage containers. BPs are endocrine disruptors； hence， they can disrupt the natural hormonal activities of the human body， impact the neurological development of children， and affect intestinal microbial communities in the body， leading to obesity. Consequently， BPs pose threats to human health. The prepared dishes are usually using plastic packaging （containers， films， tubes， etc.）； consequently， BPs migrate from the packaging material to the food in the container is hot topic of wide concern. To address this issue， an efficient， simple and accurate method for the simultaneous determination of the 15 BPs content levels in prepared dishes using ultra performance liquid chromatography-tandem mass spectrometry （UPLC-MS/MS） was developed. The effects of the extraction solvent and its proportion， the amount of weighed matrix， and type of purifying agent on the responses and recoveries of the 15 BPs were investigated under the optimized MS conditions with the aim of determining the optimal sample-preparation conditions. The prepared dishes samples were crushed and evenly mixed， after which an internal standard solution containing a mixture of bisphenols was added and dispersed using 2.0 mL of ultrapure water. Acetonitrile （8.0 mL） was subsequently added， and the sample was extracted using vortex ultrasonication， centrifuged at 10 000 r/min for 10 min， and a 3.0-mL aliquot of the centrifuged supernatant was cleaned using a Captiva EMR-Lipid clean-up column， after which the purified liquid was subjected to UPLC-MS/MS. Analyses of response values， separation effects， and chromatographic peak shapes revealed that the Waters ACQUITY HSS T
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