Evidence map›Paper›PMID 40963957›Full record

ArticleExposure and health2025

Determination of Toxic Tropane Alkaloids in Globally Sourced Soya, Cereals and Products Using Dilute-and-Shoot Technique Coupled with LC-MS/MS.

Rufielyn S Gravador, Brett Greer, Simon A Haughey, M Mar Aparicio-Muriana, Wilfred A Abia, Alexandra-Irina Mavrochefalos, Anne P Nugent, Christopher T Elliott

Abstract read
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In one paragraph

Article in Exposure and health, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

0numbers the graph read from it
0cells of the map it votes in
0citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

0 citing papers in PubMed.

No citing paper in PubMed yet.

4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

8 authors.

Rufielyn S GravadorInstitute for Global Food Security, School of Biological Sciences, Queen's University Belfast, Belfast, UK.ORCID 0000-0002-8985-4840
Brett GreerInstitute for Global Food Security, School of Biological Sciences, Queen's University Belfast, Belfast, UK.
Simon A HaugheyInstitute for Global Food Security, School of Biological Sciences, Queen's University Belfast, Belfast, UK.
M Mar Aparicio-MurianaInstitute for Global Food Security, School of Biological Sciences, Queen's University Belfast, Belfast, UK.
Wilfred A AbiaInstitute for Global Food Security, School of Biological Sciences, Queen's University Belfast, Belfast, UK.
Alexandra-Irina MavrochefalosInstitute for Global Food Security, School of Biological Sciences, Queen's University Belfast, Belfast, UK.
Anne P NugentInstitute for Global Food Security, School of Biological Sciences, Queen's University Belfast, Belfast, UK.
Christopher T ElliottInstitute for Global Food Security, School of Biological Sciences, Queen's University Belfast, Belfast, UK.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

For the first time, this study reports the content of tropane alkaloids (TAs) in soybean and soymeal samples sourced from 13 different countries, as well as in various cereals (including corn, millet, wheat, and sorghum) and a product (Super Cereals). The analysis was conducted using a fully validated solid-liquid extraction (SLE) with dilute-and-shoot (DnS) method along with a liquid chromatography-tandem mass spectrometry (LC-MS/MS) triple quadrupole system. The samples were extracted using a solution of acetonitrile and water (60:40) with 1% formic acid. The limits of quantification (LOQ) were 0.10 µg kg Supplementary Information: The online version contains supplementary material available at 10.1007/s12403-025-00718-z.

Indexed as

AtropineDilute-and-shootMatrix effectPlant toxinsScopolamineSolid-liquid extraction

Identifiers

PMID40963957
PMCPMC12436479

What OpenQuestion holds

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LicenceCC BY
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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.