Evidence map›Paper›PMID 40846681›Full record

ArticleThe Journal of organic chemistry2025

Electrochemical Dehydration of Sulfonic Acids to Their Anhydrides.

Enrico Lunghi, Annemijn M van Koten, Johannes Schneider, Siegfried R Waldvogel

Abstract read
In one paragraph

Article in The Journal of organic chemistry, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.

0numbers the graph read from it
0cells of the map it votes in
3citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

3 citing papers in PubMed.

  1. Article
  2. Review
  3. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

4 authors.

Enrico LunghiMax-Planck-Institute for Chemical Energy Conversion (MPI CEC), Stiftstraße 34-36, Mülheim an der Ruhr 45470, Germany.
Annemijn M van KotenMax-Planck-Institute for Chemical Energy Conversion (MPI CEC), Stiftstraße 34-36, Mülheim an der Ruhr 45470, Germany.
Johannes SchneiderDepartment of Chemistry, Johannes Gutenberg University (JGU), Duesbergweg 10-14, Mainz 55128, Germany.
Siegfried R WaldvogelMax-Planck-Institute for Chemical Energy Conversion (MPI CEC), Stiftstraße 34-36, Mülheim an der Ruhr 45470, Germany.ORCID 0000-0002-7949-9638

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

We developed an electrochemical method for sulfonic anhydride synthesis and one-pot derivatization into sulfonamides and mesylates under mild conditions. Aliphatic sulfonic anhydrides were electrogenerated in up to a 74% yield. Since isolating these moisture-sensitive intermediates is challenging, the in situ-generated sulfonic anhydrides were directly converted into sulfonamides or alkyl sulfonates using amines or alcohols, respectively. This scalable process enables the synthesis of various nitrogen- and oxygen-based products in the multigram range.

Identifiers

PMID40846681
PMCPMC12418306

What OpenQuestion holds

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LicenceCC BY
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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.