ArticleMolecules (Basel, Switzerland)2025
Determination of Phenylurea Herbicides in Water Samples by Magnet-Integrated Fabric Phase Sorptive Extraction Combined with High Performance Liquid Chromatography.
Article in Molecules (Basel, Switzerland), 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
In this study, a magnet-integrated fabric phase sorptive extraction (MI-FPSE) protocol was developed in combination with high pressure liquid chromatography-diode array detection (HPLC-DAD) for the simultaneous determination of five phenylurea pesticides (i.e., chlorbromuron, diuron, linuron, metoxuron, monuron) in environmental water samples. To produce the MI-FPSE device, two individual sol-gel coated carbowax 20 M (CW 20 M) cellulose membranes were fabricated and stitched to each other, while a magnetic rod was inserted between them to give the resulting device the ability to spin and serve as a stand-alone microextraction platform. The adsorption and desorption step of the MI-FPSE protocol was optimized to achieve high extraction efficiency and the MI-FPSE-HPLC-DAD method was validated in terms of linearity, sensitivity, selectivity, accuracy, and precision. The limits of detection (LODs) were found to be 0.3 μg L
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