ArticleMaterials (Basel, Switzerland)2025
Effect of Chemical Etching on the Supercapacitive Performance of Electroless Ni-B Coatings.
Article in Materials (Basel, Switzerland), 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
In our study, supercapacitor electrodes were prepared by depositing electroless Ni-B coating on copper plates, followed by nitric acid etching. The composition and the micro- and phase structure of the coatings were investigated by ICP-OES, PFIB-SEM, and XRD techniques. The original pebble-like structure of the coating consists of 0.8-10 µm particles, with an X-ray amorphous phase structure. The surface morphology and porosity of the coating can be tuned simply by changing the etching time. The supercapacitive performance of the electrodes was evaluated by means of cyclic voltammetry, galvanostatic charge-discharge, and electrochemical impedance spectroscopy measurements. The capacitance of the coating was found to vary on the etching time according to a maximum function, allowing for the determination of an optimal duration to obtain a specific capacitance of 157 mF/cm
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