Photoelectrochemistry-Promoted Ni-Catalyzed C-O Cross-Couplings.

Zhao-Ran Liu, Ye Wang, Cong Ma, Tian-Sheng Mei

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Article in Precision chemistry, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

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4 authors.

Zhao-Ran LiuState Key Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, University of Chinese Academy of Sciences, Chinese Academy of Sciences, Shanghai, 200032, China.

Ye WangState Key Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, University of Chinese Academy of Sciences, Chinese Academy of Sciences, Shanghai, 200032, China.

Cong MaState Key Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, University of Chinese Academy of Sciences, Chinese Academy of Sciences, Shanghai, 200032, China.ORCID https://orcid.org/0000-0001-7568-1347

Tian-Sheng MeiState Key Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, University of Chinese Academy of Sciences, Chinese Academy of Sciences, Shanghai, 200032, China.ORCID https://orcid.org/0000-0002-4985-1071

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

The synergistic integration of metal catalysis with electrochemistry has emerged as a powerful tool for organic synthesis. However, in nickel-catalyzed electrochemical cross-coupling reactions, mismatches between external conditions and reaction rates often lead to side reactions such as catalyst deactivation, homocoupling, and protonation. Addressing this issue through the development of strategies is highly desirable. Herein, we report the successful merging of photochemistry with electrochemistry to facilitate nickel-catalyzed C-O cross-coupling reactions, providing a practical method for the synthesis of alkyl aryl ethers. Preliminary mechanistic studies suggest that this photoelectrochemical strategy effectively enhances the efficiency of nickel-catalyzed C-O cross-coupling reactions compared to traditional electrochemical methods by regenerating the active Ni

Indexed as

alkyl aryl etherC−O cross-couplingnickel catalysispaired electrolysisphotoelectrochemistry

Identifiers

PMID40746585

DOI10.1021/prechem.5c00015

PMCPMC12308595

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