Evidence map›Paper›PMID 40628786›Full record

ArticleScientific reports2025

Preparation and characterization of bio-waste derived chitosan/hydroxyapatite/pectin green biocomposite.

Sara Etminanrezaeieh, Khadije Rezazadeh, Elham Jalilnejad, Reza Rafiee

Erratum issuedAbstract read
In one paragraph

Article in Scientific reports, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. An erratum has been issued. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Article
  2. Article
4 · The record

Corrections and comments

5 · Who and what money

Authors and funding

4 authors.

Sara EtminanrezaeiehFaculty of Chemical Engineering, Urmia University of Technology, Urmia, Iran.
Khadije RezazadehFaculty of Chemical Engineering, Urmia University of Technology, Urmia, Iran.
Elham JalilnejadFaculty of Chemical Engineering, Urmia University of Technology, Urmia, Iran.
Reza RafieeFaculty of Chemical Engineering, Urmia University of Technology, Urmia, Iran. reza.rafiee@uut.ac.ir.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

This study focuses on the synthesis and structural analysis of biocomposites comprising chitosan (Cs), hydroxyapatite (HA), and pectin (Pe). Cs was extracted from shrimp skin, HA from bovine teeth and bones, and Pe from orange peel and apple. The biocomposites were prepared via a freeze-drying method using glutaraldehyde (GA) as a cross-linking agent. FTIR, XRD, FE-SEM, EDS-EDAX and BET were employed to characterize the chemical structure, crystallinity, morphology, surface area, and elemental composition. The extracted Cs had a molecular weight of 4.1 × 10⁵ Da, a 70% degree of deacetylation, and an extraction yield of 31.2%. The results confirmed biocomposite formation with a near-stoichiometric Ca/P ratio (1.67) in HA. Biocomposites containing HA calcined at 1000 °C and Pe from orange peel with 72% galacturonic acid, exhibited enhanced crystallinity (up to 70.61%), uniform dispersion, and high porosity. While an increased HA content improved morphology and surface area (up to 12.5 m

Indexed as

Biocompatible MaterialsChitosanDurapatitePectinsAnimalsCattleCitrus sinensisSpectroscopy, Fourier Transform InfraredX-Ray DiffractionBiocompatible MaterialsChitosanDurapatitePectinsBiocompositeChitosanFreeze-dryingHydroxyapatitePectin

Identifiers

PMID40628786
PMCPMC12238635

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.