Evidence map›Paper›PMID 40627349›Full record

ArticleACS nano2025

Spatially Resolved In Situ X-ray Absorption Spectroscopy Studies of ZnS Nanoparticle Synthesis at the Water-Toluene Interface.

Lars Klemeyer, Francesco Caddeo, Tjark L R Gröne, Sani Y Harouna-Mayer, Brian Jessen, Cecilia A Zito, Jagadesh Kopula Kesavan, Ann-Christin Dippel, Fernando Igoa Saldaña, Olivier Mathon and 2 more

Abstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in ACS nano, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Article
  2. Journal of the American Chemical Society · 2025
    Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

12 authors.

Lars KlemeyerInstitute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures, University of Hamburg, Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0000-0003-1103-8103
Francesco CaddeoInstitute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures, University of Hamburg, Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0000-0002-2909-5379
Tjark L R GröneInstitute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures, University of Hamburg, Luruper Chaussee 149, 22761 Hamburg, Germany.
Sani Y Harouna-MayerInstitute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures, University of Hamburg, Luruper Chaussee 149, 22761 Hamburg, Germany.
Brian JessenInstitute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures, University of Hamburg, Luruper Chaussee 149, 22761 Hamburg, Germany.
Cecilia A ZitoInstitute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures, University of Hamburg, Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0000-0001-5596-012X
Jagadesh Kopula KesavanInstitute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures, University of Hamburg, Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0000-0002-0591-2493
Ann-Christin DippelDeutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg, Germany.
Fernando Igoa SaldañaDeutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg, Germany.
Olivier MathonESRF, The European Synchrotron, 38043 Grenoble, France.
Pieter GlatzelESRF, The European Synchrotron, 38043 Grenoble, France.ORCID 0000-0001-6532-8144
Dorota KoziejInstitute for Nanostructure and Solid-State Physics, Center for Hybrid Nanostructures, University of Hamburg, Luruper Chaussee 149, 22761 Hamburg, Germany.ORCID 0000-0002-9064-2642

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Two-phase synthesis is a well-established approach for achieving precise control of the nanoparticle properties. However, studying and understanding chemical transformations in such a spatially heterogeneous system is challenging. In this work, we introduce a two-phase synthesis route for ZnS nanoparticles (ZnS NPs) at the water-toluene interface. By employing spatially resolved in situ high-energy resolution fluorescence-detected X-ray absorption spectroscopy (HERFD-XAS) combined with density functional theory (DFT) calculations, we track the diffusion of Zn

Indexed as

focused X-ray spectroscopyHERFD-XANESnanoparticle synthesisnucleation and growthtwo-phase synthesisX-ray total scatteringzinc sulfide

Identifiers

PMID40627349
PMCPMC12291586

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.