Evidence map›Paper›PMID 40616138›Full record

ArticleBMC chemistry2025

Efficient mechanochemical synthesis of new fluorinated Schiff bases: a solvent-free, alternative to conventional method with mercury adsorption properties.

Mirza T Baig, Mariam T Sayed, Reem Aledamat, Sumyah Hassan, Alaa AlReyashi, Naheed Sidiq, Siham Y Al-Qaradawi, Mohamed F Mady

Abstract read
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Article in BMC chemistry, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Article
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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

8 authors.

Mirza T BaigDepartment of Chemistry and Earth Sciences, College of Arts and Sciences, Qatar University, Doha, Qatar.
Mariam T SayedDepartment of Chemistry and Earth Sciences, College of Arts and Sciences, Qatar University, Doha, Qatar.
Reem AledamatDepartment of Chemistry and Earth Sciences, College of Arts and Sciences, Qatar University, Doha, Qatar.
Sumyah HassanDepartment of Chemistry and Earth Sciences, College of Arts and Sciences, Qatar University, Doha, Qatar.
Alaa AlReyashiDepartment of Chemistry and Earth Sciences, College of Arts and Sciences, Qatar University, Doha, Qatar.
Naheed SidiqDepartment of Chemistry and Earth Sciences, College of Arts and Sciences, Qatar University, Doha, Qatar.
Siham Y Al-QaradawiDepartment of Chemistry and Earth Sciences, College of Arts and Sciences, Qatar University, Doha, Qatar.
Mohamed F MadyDepartment of Chemistry and Earth Sciences, College of Arts and Sciences, Qatar University, Doha, Qatar. mmady@qu.edu.qa.

Funding

Qatar National Research Fund UREP 30-088-3-028
6 · The paper itself

Abstract

The development of sustainable synthetic techniques is of critical importance in modern chemistry. This paper describes a mechanochemical approach to the synthesis of novel fluorinated Schiff bases via ball milling, which provides a fast, high-yield, and green alternative to conventional reflux methods. The synthesized fluorinated Schiff bases are evaluated for their adsorption capacity and efficiency in mercury removal and compared to assess their performance, demonstrating that ball milling produced compounds with comparable physical attributes to those produced via traditional solvent-based procedures. However, ball milling considerably shortened reaction time, with some reactions taking less than 5 min, and enhanced yields, reaching up to 92%, which is significantly higher than that achieved by conventional methods. The molecular structure of the synthesised Schiff bases is validated using analytical and spectroscopic techniques, including

Indexed as

Ball millingFluorine organo-compoundsGreen chemistryMercury adsorptionSchiff basesSolvent-free reaction

Identifiers

PMID40616138
PMCPMC12231667

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.